Packed Bed Reactor Apparatus

Packed Bed Reactor Apparatus

The setup consists of a glass column packed with Rasching Rings and two feed tanks. Reactants are fed to the reactor through a liquid distributor, fitted at the bottom of the column. Rotameters are provided to measure the individual flow of Chemicals. The flow rate can be adjusted by operating the needle valves provided on the respective Rotameter.


Description

The setup consists of a glass column packed with Rasching Rings and two feed tanks. Reactants are fed to the reactor through a liquid distributor, fitted at the bottom of the column. Rotameters are provided to measure the individual flow of Chemicals. The flow rate can be adjusted by operating the needle valves provided on the respective Rotameter. Compressed air is used for the circulation of feed. Samples can be taken periodically from the top outlet of the reactor. Pressure Regulator & Pressure Gauge are fitted in the compressed airline

Experimentation/Learning Objectives
• Saponification Reaction studies in Packed Bed Reactor.
• To determine the Reaction Rate Constant.

Utilities Required
• Compressed Air Supply: 0.5 [email protected] bar
• Water Supply.
• Floor Drain.
• Floor Area Required : 1.0 m x 1.0 m.
• Instruments, Laboratory Glassware and Chemicals required for analysis as per the system adopted

Reactor Column: Material Borosilicate Glass Volume 1.2 Ltrs. (Approx).
• Packing: Ranching Rings, Material Borosilicate Glass. Size 6-8 mm (approx)
• Feed Tank (2Nos.): Material Stainless Steel, Capacity 20 Ltrs.
• Feed Circulation: By compressed air.
• Flow Measurement: Rotameter 2Nos. (One each for Reactants).
• Piping: Stainless Steel and PU Pipe.
• Pressure Regulator : 0-2 Kg/cm2
• Pressure Gauge: Bourdon type 0-2 Kg/cm2
• An ENGLISH instruction manual consisting of experimental procedures, block diagram, etc. will be provided along with the Apparatus.
• The whole set-up is well designed and arranged on a rigid structure painted with industrial PU Paint.

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